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- W2898845303 abstract "Abstract Two synthetic models of the active site of [FeFe]‐hydrogenase containing mixed (S, Se) and (S, Te) bridges have been synthesized and characterized. These complexes [Fe 2 ( CO ) 6 {μ‐S( CH 2 ) 4 E‐μ)}] (E = Se ( 1 ), Te ( 2 )) are obtained in moderate yields from the reaction of Fe 3 ( CO ) 12 with 1,2‐thiaselenane or 1,2‐thiatellurane. They have been characterized by spectroscopic techniques ( IR , 1 H‐, 13 C{ 1 H}‐, 77 Se{ 1 H}‐, 125 Te{ 1 H}‐ NMR , and MS ) and elemental analysis. The structures of [Fe 2 ( CO ) 6 {μ‐S( CH 2 ) 4 Se‐μ)}] and [Fe 2 ( CO ) 6 {μ‐S( CH 2 ) 4 Te‐μ)}] are determined by X‐ray structure determination and show the expected butterfly geometry. Moreover, the influence of the mixed chalcogen atoms on the redox properties and the catalytic behavior of 1 and 2 are studied using cyclic voltammetry." @default.
- W2898845303 created "2018-11-09" @default.
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- W2898845303 date "2018-10-30" @default.
- W2898845303 modified "2023-09-25" @default.
- W2898845303 title "[FeFe]-hydrogenase H-cluster mimics mediated by mixed (S, Se) and (S, Te) bridging moieties: Insight into molecular structures and electrochemical characteristics" @default.
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- W2898845303 doi "https://doi.org/10.1002/hc.21446" @default.
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