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- W2898884037 abstract "Transparent organic-inorganic hybrid films with composition (wt%) PVA(54,5): PEG(40): B2O3(5,5) is obtained by the sol-gel process and solution casting method at ambient temperature. Two different precursors of boron aqua solutions of boric acid (H3BO3) and ethanol solution of trimethyl borate (СН3О)3В) are used for the preparation of hybrid solutions. The effect of starting boron solution type on the structure of obtained materials are studied by infrared spectroscopy (IR). It was found that degree of cross-linking and type of bonding in the hybrid structure are depended on by the functionality of borate units. From experimental and calculated spectral data it can be concluded that the best cross-linked hybrid structure is obtained from the aqua solution of H3BO3 at pH 10, with a predominant amount of polyborate ions involved in the B-O-C ester complexes. By combined experimental and computational study, a probable mechanism of boron-containing organic-inorganic network are proposed." @default.
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- W2898884037 date "2018-03-01" @default.
- W2898884037 modified "2023-09-26" @default.
- W2898884037 title "Polymer - borate hybrids films - theoretical and experimental dеtermination of the structure" @default.
- W2898884037 doi "https://doi.org/10.29167/a1i1p184-190" @default.
- W2898884037 hasPublicationYear "2018" @default.
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