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• W2898981889 abstract "Abstract A novel thulium p -hydroxybenzenesulfonate complex [Tm(C 6 H 5 O 4 S) 2 (H 2 O) 6 ](C 6 H 5 O 4 S)·3H 2 O ( 1 ) was solvothermally synthesized and characterized by elemental analyses, photoluminescence, solid-state UV/vis diffuse reflectance, magnetic measurements and single-crystal X-ray diffraction. Complex 1 features an ionic structure with the thulium ion possessing a square antiprismatic geometry. Complex 1 crystallized in the monoclinic system with space group P 2 1 . Photoluminescent measurements with solid-state sample demonstrate that the anti-Stokes emission bands in the red/NIR spectral region 710 and 812 nm are observed from the Tm 3+ 4f intrashell transitions from the 3 F 2,3 excited states to the 3 H 6 and 1 G 4 excited state to the 3 H 5 state, respectively. Solid-state UV/vis diffuse reflectance spectra of complex 1 show the existence of a wide optical band gap of 3.56 eV. Variable-temperature magnetic susceptibility and field dependence magnetization measurements are also studied and the magnetic susceptibility obeys the Curie-Weiss law ( χ m = c /( T − θ )) with the value C being of 8.6 K and a negative Weiss constant θ being of −0.2 K." @default.
• W2898981889 created "2018-11-09" @default.
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• W2898981889 date "2018-10-25" @default.
• W2898981889 modified "2023-09-27" @default.
• W2898981889 title "Synthesis, structure, photoluminescent, optical and magnetic properties of a novel thulium p-hydroxybenzenesulfonate complex" @default.
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• W2898981889 doi "https://doi.org/10.1515/zkri-2017-2105" @default.
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