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- W2899283106 abstract "In this work, we report the catalytic performance of a MoO2Cl2 anchored metal-organic framework, [email protected], in the oxidative desulfurization (ODS) process on a continuous fixed-bed reactor. [email protected] was examined as a catalyst in the oxidation of model oils containing dibenzothiophene (DBT), benzothiophene (BT) or 4,6-dimethyldibenzothiophene (4,6-DMDBT). In a 50-h ODS reaction of DBT at 70 °C, with tert-butyl hydroperoxide (TBHP) as the oxidant, a constant high DBT conversion of nearly 80% was observed along with a high oxidant utility of over 85%, where DBT was converted rapidly into DBT sulfone. XRD and ICP analysis show that the structure of [email protected] was well preserved, with no significant leaching of Mo species. In addition, [email protected] can also oxidize a hydrogenated diesel oil, and 74% sulfur removal efficiency was achieved, with an extraction recovery of 92.5% after acetonitrile extraction. Spectroscopic characterization confirmed the formation of a molybdenum peroxide complex from MoO2Cl2 under TBHP treatment, a plausible catalytic process was proposed based on the experiment evidence as well as FT-IR and FT-FIR characterization results." @default.
- W2899283106 created "2018-11-09" @default.
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- W2899283106 date "2019-03-01" @default.
- W2899283106 modified "2023-10-16" @default.
- W2899283106 title "Catalytic oxidative desulfurization of model and real diesel over a molybdenum anchored metal-organic framework" @default.
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- W2899283106 doi "https://doi.org/10.1016/j.micromeso.2018.11.004" @default.
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