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• W2899445627 abstract "Amorphous calcium phosphate (ACP) is essential in formation of mineralized bone and using as a bone substitute. This study presents new aspects of carbonated ACP crystallization during heat treatment. Initially synthesis end pH and drying method (80 °C or freeze-drying) of ACP were varied. Thermal behaviour and structure of differently obtained ACP were evaluated using DSC-TGA, heating microscopy, XRD, FT-IR. In addition, degree of crystallinity (DOC), phase composition and chemical group information were compared for as-synthesized and heat-treated (crystallization end T and 1200 °C) ACP. For the first time DSC-TGA and heating microscopy methods were correlated. DOC of samples dried at 80 °C was synthesis end pH dependent. Heat treatment without temperature hold at crystallization end T produced materials with DOC of 82–91%, thus proving efficiency of low temperature processing. Variations in drying method and synthesis end pH affect structure of the samples heat treated at crystallization end T, but not at 1200 °C." @default.
• W2899445627 created "2018-11-09" @default.
• W2899445627 creator A5060452646 @default.
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• W2899445627 date "2019-04-01" @default.
• W2899445627 modified "2023-10-02" @default.
• W2899445627 title "Amorphous calcium phosphate materials: Formation, structure and thermal behaviour" @default.
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• W2899445627 doi "https://doi.org/10.1016/j.jeurceramsoc.2018.11.003" @default.
• W2899445627 hasPublicationYear "2019" @default.
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