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- W2899541054 abstract "We report on the size dependence of the Ag–Cu nano-alloy melting temperatures via differential scanning calorimetry (DSC) measurements of silica-coated Ag–Cu nanoparticles (NPs) and the thermodynamic modeling. Four Ag–Cu alloy NP samples with compositions ranging from Ag8Cu2 to Ag5Cu5 were prepared via NaBH4 co-reduction and silica-coating. The experimental size dependence of melting temperature was obtained via UV–visible absorption spectra, transmission electron microscopy, and DSC. On the basis of the measured melting temperatures of the Ag–Cu nano-alloys in this work as well as the thermodynamic properties of the pure Ag and Cu NPs and Ag–Cu systems in literature, the theoretically calculated size dependence of Ag–Cu NP melting temperatures was then obtained via thermodynamic modeling of the Ag–Cu nano-system. Thermodynamically calculated size dependence of the melting temperatures for Ag–Cu alloy NPs shows a nonlinear function with respect to the inverse of the particle size and satisfactory agreement with experimental observations. This work establishes a methodology for determining the melting temperature as a function of size for different nano-alloy systems." @default.
- W2899541054 created "2018-11-16" @default.
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- W2899541054 date "2018-11-06" @default.
- W2899541054 modified "2023-10-10" @default.
- W2899541054 title "Nonlinear Size-Dependent Melting of Silica-Encapsulated Ag–Cu Alloy Nanoparticles" @default.
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- W2899541054 doi "https://doi.org/10.1021/acs.jpcc.8b09156" @default.
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