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- W2899700658 abstract "Among transition metal oxides, MnO2 is of considerable importance for various technological end-uses, from heterogeneous catalysis to gas sensing, owing to its structural flexibility and unique properties at the nanoscale. In this work, we demonstrate the successful fabrication of supported MnO2 nanomaterials by a catalyst-free, plasma-assisted process starting from a fluorinated manganese(II) molecular source in Ar/O2 plasmas. A thorough multitechnique characterization aimed at the systematic investigation of material structure, chemical composition, and morphology revealed the formation of F-doped, oxygen-deficient, MnO2-based nanomaterials, with a fluorine content tunable as a function of growth temperature (TG). Whereas phase-pure β-MnO2 was obtained for 100 °C ≤ TG ≤ 300 °C, the formation of mixed phase MnO2 + Mn2O3 nanosystems took place at 400 °C. In addition, the system nano-organization could be finely tailored, resulting in a controllable evolution from wheat-ear columnar arrays to high aspect ratio pointed-tip nanorod assemblies. Concomitantly, magnetic force microscopy analyses suggested the formation of spin domains with features dependent on material morphology. Preliminary tests in Vis-light activated photocatalytic degradation of rhodamine B aqueous solutions pave the way to possible applications of the target materials in wastewater purification." @default.
- W2899700658 created "2018-11-16" @default.
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- W2899700658 date "2018-11-08" @default.
- W2899700658 modified "2023-10-18" @default.
- W2899700658 title "Insights into the Plasma-Assisted Fabrication and Nanoscopic Investigation of Tailored MnO<sub>2</sub> Nanomaterials" @default.
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- W2899700658 doi "https://doi.org/10.1021/acs.inorgchem.8b02108" @default.
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