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- W2899804704 abstract "Treatment of [1,4-(PhS)2C6H4] and [1,2-(PhS)2C6H4] with the appropriate amount ofO-mesitylenesulfonylhydroxylamine (MSH) yields the corresponding protonatedsulfimides, both of which may be deprotonated with 1,8-diazabicyclo[5.4.0]undec-7-ene (DBU) to give the hydrated free sulfimides [1,4-(PhS{NH2})2C6H4] and [1,2-(PhS{NH2})C6H4PhS]. It would seem that both products display the ability to givetwo distinct types of material, anhydrous and hydrated forms. The hydrated type [1,4-(PhS{NH2})2C6H4].2H2O has been found by crystallography to form an extendedarray system; whereas the crystal structure of the dehydrate exhibits extra structuralrigidity brought about by having two hydrogen-bonded sulfimide units permolecule. The ligand [1,2-(PhS{NH2})C6H4PhS] also exhibits two distinct types offormation, one a dehydrate (exhibited as an oil) and the other a hydrated type (presentas a crystalline solid). [Continues.]" @default.
- W2899804704 created "2018-11-16" @default.
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- W2899804704 date "2003-01-01" @default.
- W2899804704 modified "2023-09-23" @default.
- W2899804704 title "Preparation and coordination chemistry of novel derivatised sulfimides" @default.
- W2899804704 hasPublicationYear "2003" @default.
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