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- W2901431330 abstract "Abstract Recently, 5‐hydroxymethyl furfural (5‐HMF) became into the spotlight as one of the most promising biorenewable platforms available from carbohydrates. Among other versatile derivatives of 5‐HMF its dimer 5,5′‐(oxy‐bis (methylene)) bis‐2‐furfural (OBMF) was recognized as a useful building block for the production of polymers and pharmaceuticals. Herein we explored the synthesis of OBMF under solvent free conditions applying vacuum as a green tool for water removal. Several readily available acidic resins, silica gel supported inorganic acid, acidic zeolites and Lewis acids were studied as promoters for this transformation. Under these conditions, SiO 2 /CF 3 SO 3 H exhibited the best performance allowing the synthesis of OBMF in 55 % yield in only 1 min reaction time. Similar results were achieved using Amberlyst 15 and SO 2 /PPA resulting in 51 % yield in 20 min and 46 % yield in 10 min, respectively." @default.
- W2901431330 created "2018-11-29" @default.
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- W2901431330 date "2018-11-20" @default.
- W2901431330 modified "2023-10-01" @default.
- W2901431330 title "Solvent‐Free Catalytic Self‐Etherification of 5‐Hydroxymethyl Furfural" @default.
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- W2901431330 doi "https://doi.org/10.1002/cctc.201801560" @default.
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