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• W2901474005 abstract "Continuous hydrogenation using ACMC-Pd monolith catalysts was studied for four chemistries of industrial interest. The chemistry was run in a 30.5 cm catalyst bed with repeated passes to simulate a longer commercial catalyst bed in which >97% conversion would be completed in a single pass of the reactor with no recycle. The selected liquid flow rate (0.086 cm/s) enabled >97% conversion for the four chemistries using practical ranges of temperature (60–180 °C), pressure (0.348 to 3.48 MPa), and required bed lengths (4.3 to 6.1 m). The unsaturated bonds hydrogenated included nitro, carbonyl, olefin, and aromatic bond types. The most challenging reaction was the conversion of a neat olefinic/aromatic substrate (requiring 7 moles of hydrogen per mole of product) run with a low-temperature/high-temperature reactor configuration. The same catalyst was used for all of the chemistries, and the changeover from one chemistry to another involved simple solvent/substrate rinses of the reactor. The data can be used to estimate the number of commercial reactor tubes, temperature, pressure, and bed length needed for the production of commercial quantities of specialty and pharmaceutical chemicals." @default.
• W2901474005 created "2018-11-29" @default.
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• W2901474005 date "2018-11-20" @default.
• W2901474005 modified "2023-09-30" @default.
• W2901474005 title "Run Parameters for a Continuous Hydrogenation Process Using ACMC-Pd To Replace Commercial Batch Reactor Processes" @default.
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• W2901474005 doi "https://doi.org/10.1021/acs.oprd.8b00286" @default.
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