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• W2901477671 endingPage "7602" @default.
• W2901477671 startingPage "7598" @default.
• W2901477671 abstract "A synthesis of the nonreducing end hexasaccharide of saccharomicin B, α-l-Eva-(1→4)-α-l-Eva-(1→4)-α-l-Dig-(1→4)-α-l-Eva-(1→4)-α-l-Dig-(1→4)-β-d-Fuc, has been developed. Selective glycosylations of l-digitoxose (l-Dig) using AgPF6/TTBP-mediated thioether activation and l-4-epi-vancosamine (l-Eva) using Tf2O/DTBMP-mediated sulfoxide activation produced the hexasaccharide as a single diastereomer in very good yield. This hexasaccharide is properly functionalized to serve as a glycosyl donor for the total synthesis of saccharomicin B." @default.
• W2901477671 created "2018-11-29" @default.
• W2901477671 creator A5005887397 @default.
• W2901477671 creator A5009403356 @default.
• W2901477671 date "2018-11-14" @default.
• W2901477671 modified "2023-10-18" @default.
• W2901477671 title "Synthesis of the Non-Reducing Hexasaccharide Fragment of Saccharomicin B" @default.
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• W2901477671 doi "https://doi.org/10.1021/acs.orglett.8b03333" @default.
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