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• W2901809766 abstract "Abstract An eco‐friendly catalytic system consisted of dihydric phosphate (H 2 PO 4 — ) catalyst and a methyl isobutyl ketone (MIBK)/H 2 O biphasic solvent has been constructed to produce 5‐hydroxymethylfurfural (HMF) from sucrose, a cheaper and more widely available feedstock than fructose. The effects of reaction conditions, viz ., catalyst dosage, reaction temperature, and reaction time, on this dehydration reaction have been investigated systematically, affording more than 70% of HMF yield under the optimum conditions. This environmentally friendly system is also broadly substrate‐tolerant, high concentration of sucrose (86%), scalable catalytic system (scaled up 10 times), and sugarcane juice also give 62.5%, 70.1%, and 70.7% of HMF yield, respectively. Moreover, the function of H 2 PO 4 — containing system for isomerization of glucose into fructose has been confirmed; and the dehydration reaction has been proposed to proceed through the catalytic hydrolysis of sucrose into glucose and fructose by protons (H + ), followed by the isomerization of glucose into fructose by hydrogen phosphate ions (HPO 4 2− ), and the dehydration of fructose into HMF by protons (H + ), which are all from the dissociation of H 2 PO 4 — ions. Readily available and eco‐friendly catalyst, abundantly available feedstock, and simple reaction conditions could mark this process promising for HMF production in industry." @default.
• W2901809766 created "2018-11-29" @default.
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• W2901809766 date "2018-11-19" @default.
• W2901809766 modified "2023-09-25" @default.
• W2901809766 title "Eco‐Friendly Production of 5‐Hydroxymethylfurfural from Sucrose Using Commercially Available Dihydric Phosphate as a Catalyst" @default.
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• W2901809766 doi "https://doi.org/10.1002/slct.201801814" @default.
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