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• W2902364120 abstract "Eight new members of two series of PEG-6000-bridged geminal dicationic ionic liquids based on diphenylammonium/imidazolium cation were synthesized by the change of four anions $$hbox {CF}_{3}hbox {COO}^{-}$$ , $$hbox {CCl}_{3}hbox {COO}^{-}$$ , $$hbox {AcO}^{-}$$ and $$hbox {HSO}_{4}^{-}$$ . They were investigated as reusable acidic catalysts for dehydration of fructose to 5-hydroxymethylfurfural in polar aprotic solvent. The characterizations of dicationic ionic liquids were done using $${}^{1}hbox {H NMR}$$ , $${}^{13}hbox {C NMR}$$ , IR and TGA analyses. Irrespective of Hammett acidity strength of the eight ILs, they displayed single peak selectivity for the 5-hydroxymethyl furfural intermediate in HPLC analysis. Two series of N-sulfonic acid functionalized PEG-6000 bridged geminal dicationic diphenylammonium/imidazolium ionic liquids were developed in pair with $$hbox {CF}_{3}hbox {COO}^{-}$$ , $$hbox {CCl}_{3}hbox {COO}^{-}$$ , $$hbox {AcO}^{-}$$ and $$hbox {HSO}_{4}^{-}$$ anions. Single peak selectivity of 5-hydroxymethylfurfural in HPLCs was observed from dehydration of fructose in polar aprotic solvent using these acidic ionic liquid catalysts." @default.
• W2902364120 created "2018-12-11" @default.
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• W2902364120 date "2018-11-30" @default.
• W2902364120 modified "2023-09-26" @default.
• W2902364120 title "Investigation of PEG-6000 bridged $$hbox {-N-SO}_{3}hbox {H}$$ -N-SO 3 H functionalized geminal dicationic ionic liquids for catalytic conversion of fructose to 5-hydroxymethylfurfural" @default.
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• W2902364120 doi "https://doi.org/10.1007/s12039-018-1570-9" @default.
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