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- W2903232667 startingPage "192" @default.
- W2903232667 abstract "Anchoring of peroxidovanadium(V) (pV) species to chitosan, a natural chelating polymer, afforded a new and structurally defined immobilized complex, VO(O2)2(NH2)-chitosan (ChpV) which was comprehensively characterized by elemental analysis (CHN, ICP-OES, energy dispersive X-ray spectroscopy), spectral studies (FT-IR, Raman, 13C NMR, diffuse reflectance UV–Vis and XPS), SEM, XRD, Brunauer–Emmett–Teller (BET) and thermogravimetric analysis (TGA). Apart from being thermally stable, the compound is water-tolerant and non-hygroscopic. The compound effectively facilitated chemoselective oxidation of thioethers with H2O2 in aqueous medium to the respective high purity sulfoxide, in impressive yield (TOF 5628 h−1) and with high H2O2 efficiency, under mild reaction condition. In addition to water, the heterogeneous catalyst is highly compatible in a variety of organic solvents and is recyclable for several catalytic cycles without significant loss in selectivity. The catalytic procedure is amenable to ready scalability and is free from halogen, co-catalyst and acidic or any other hazardous additive." @default.
- W2903232667 created "2018-12-11" @default.
- W2903232667 creator A5019083561 @default.
- W2903232667 creator A5053161172 @default.
- W2903232667 creator A5067364030 @default.
- W2903232667 creator A5069739124 @default.
- W2903232667 creator A5073390101 @default.
- W2903232667 creator A5079651011 @default.
- W2903232667 date "2019-02-01" @default.
- W2903232667 modified "2023-10-18" @default.
- W2903232667 title "A chitosan supported peroxidovanadium(V) complex: Synthesis, characterization and application as an eco-compatible heterogeneous catalyst for selective sulfoxidation in water" @default.
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