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- W2903324013 abstract "[Bis(acetylacetonato)manganese(II)] complexes are important precursors for the synthesis of catalytic MnO nanoparticles. However, the mechanism of the formation of these materials still remains unknown. In this work, a combination of ex situ and synchrotron‐based in situ powder X‐ray diffraction with in situ pH, conductivity, and turbidity measurements was applied to investigate the concentration‐dependent formation of [Mn(acac) 2 (H 2 O) 2 ]; interestingly [Mn(acac) 2 (H 2 O) 2 ] undergoes an expansion of the unit cell during the synthesis as well as upon heating. Increasing the temperature to 80 °C caused the conversion of solid [Mn(acac) 2 (H 2 O) 2 ] to the trimer compound [Mn(acac) 2 ] 3 , which occurs ex situ (in solid state), but is hindered in solution. [Mn(acac) 2 (H 2 O) 2 ] emits light in the blue‐green spectral range with emission maximum at 520 nm, measured in situ under real reaction conditions during its formation due to the instability of this compound." @default.
- W2903324013 created "2018-12-11" @default.
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- W2903324013 date "2018-11-29" @default.
- W2903324013 modified "2023-09-25" @default.
- W2903324013 title "In situ Monitoring of the Formation of [Bis(acetylacetonato)manganese(II)] Complexes" @default.
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- W2903324013 doi "https://doi.org/10.1002/zaac.201800392" @default.
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