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- W2904145110 abstract "The reductive extraction behavior of Ln (Ce,Sm) and its on-line monitoring were explored in LiClKCl/BiLi system. According to calibration curve, the relationship of peak current and concentration of Ln (Ce,Sm) measured by square wave voltammetry, the calculated Ln (III) concentration is almost consistent with that analyzed by ICP-AES, and the relative average error is about 5.37%. The effects of Li content in BiLi alloys, temperature and stirring speed on extraction rates, efficiencies and distribution ratios for Ce and Sm were determined, and found that the extraction rates, efficiencies and distribution ratios for Ce and Sm increase with the increasing the temperature, content of Li in BiLi alloys and stirring speed. The extraction rates and efficiencies for Ln from LiClKClLnCl3 molten salts are higher than those for Ln from LiClKClCeCl3SmCl3 molten salts, and the ones for Ce are much larger than those for Sm due to the formation of Sm (II) checked using XPS and linear sweep voltammetry. The produced Sm (II) could consume some reduced Sm metal: 2Sm(III)+Sm=3Sm(II), resulting in the decrease of the extraction rate, efficiency and distribution ratios of Sm. The experimental results showed the feasibility of on-line monitoring of reductive extraction process of Ln in LiCL-KCl/BiLi system by electrochemical technique." @default.
- W2904145110 created "2018-12-22" @default.
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- W2904145110 date "2019-02-01" @default.
- W2904145110 modified "2023-10-13" @default.
- W2904145110 title "Reductive extraction of lanthanides (Ce,Sm) and its monitoring in LiCl KCl/Bi Li system" @default.
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- W2904145110 doi "https://doi.org/10.1016/j.jnucmat.2018.12.010" @default.
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