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- W2904253412 abstract "This paper details synthesis methods that were used to fabricate phase-pure Nd3BSi2O10 using a LiCl-flux method. In this study, a variety of conditions were evaluated to find the optimal processing parameters for maximizing the Nd3BSi2O10 yield including the mass ratio of LiCl to target mass of Nd3BSi2O10 (i.e., 1:3, 1:2, 1:1, 2:1, and 6:1) as well as the soak temperature (i.e., 700, 800, or 900 °C) at the 1:1 ratio. It was found that the optimal ratio of LiCl:Nd3BSi2O10 was 1:1 and the optimal heat-treatment temperature was 900 °C (of those temperatures evaluated). Product made from the 1:1 material synthesized at 900 °C was recovered and fired at temperatures of 925–1350 °C. After 4-h firings at temperatures of 925–1100 °C, the Nd3BSi2O10 phase purity was found to be 100% with powder X-ray diffraction, but started to decompose at the longer firing times at 1100 °C and higher temperatures (1350 °C) at the 4-h dwell time. Thus, the lowest firing temperature for achieving a phase-pure pellet was 925 °C under the conditions studied here. The phase-pure sample was found to contain 28 vol% open porosity determined by Archimedes’ method. The durability of the Nd3BSi2O10 product was examined in flow-through conditions at 90 °C with contacting solution between pH90ºC 4.1 and 10.1. The release rate of Nd from the material had a maximum at pH90ºC 4.1 calculated to be 4.93 g m−2 d−1 and a minimum release rate of Nd at pH90ºC 7.7 of <1.34 × 10−5 g m−2 d−1. These release rates are roughly three orders of magnitude lower than what is normally measured from typical glass waste forms at pHs of 7–9." @default.
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- W2904253412 date "2019-03-01" @default.
- W2904253412 modified "2023-10-18" @default.
- W2904253412 title "Synthesis of Nd3BSi2O10 using a LiCl-flux method" @default.
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- W2904253412 doi "https://doi.org/10.1016/j.jnucmat.2018.12.016" @default.
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