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• W2904319238 abstract "A new synthesis protocol for the preparation of hitherto unknown 1′,5′-anhydro-4′-amino-trityl/MMTr hexitol nucleosides has been developed. Key steps in the synthesis of the pyrimidine analogues (U and C) include the regioselective d-allo-hexitol oxirane and 2′,4′-anhydronucleoside ring opening by uracil and azide, respectively. A different strategy using a regioselective epoxide ring opening of d-gulo-oxirane, followed by a SN2 type of azidation reaction, has been adopted for the purine analogues (A and G). These compounds can be easily converted to 6′-phosphoramidites for the solid-phase synthesis of N4′ → P6′ phosphoramidates of amino hexitol nucleic acids (AHNA)." @default.
• W2904319238 created "2018-12-22" @default.
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• W2904319238 date "2018-12-07" @default.
• W2904319238 modified "2023-10-18" @default.
• W2904319238 title "Synthesis of Protected Amino Hexitol Nucleosides as Building Blocks for Oligonucleotide Synthesis" @default.
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• W2904319238 doi "https://doi.org/10.1021/acs.joc.8b02444" @default.
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