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- W2904371746 abstract "Enantioenriched 2-aryl azepanes and 2-arylbenzazepines were generated biocatalytically by asymmetric reductive amination using imine reductases or by deracemization using monoamine oxidases. The amines were converted to the corresponding N′-aryl ureas, which rearranged on treatment with base with stereospecific transfer of the aryl substituent to the 2-position of the heterocycle via a configurationally stable benzyllithium intermediate. The products are previously inaccessible enantioenriched 2,2-disubstituted azepanes and benzazepines." @default.
- W2904371746 created "2018-12-22" @default.
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- W2904371746 date "2018-12-06" @default.
- W2904371746 modified "2023-10-12" @default.
- W2904371746 title "Chemoenzymatic Synthesis of Substituted Azepanes by Sequential Biocatalytic Reduction and Organolithium-Mediated Rearrangement" @default.
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- W2904371746 doi "https://doi.org/10.1021/jacs.8b11891" @default.
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