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• W2905027424 abstract "It is proposed a new approach to evaluate the performance of ultraviolet photoreactions by integrating UV-LED and a UV-Vis cuvette as a mini-reactor for kinetic monitoring in a spectrophotometer not influenced by external light. This system uses only 3.0 mL of solutions in a rectangular quartz cuvette with a mini-bar magnetic stirrer in a cell holder and a UV-LED of 5 W with λmax at 370 nm was positioned on the top of the cuvette and maintained at 25.0 oC. The effectiveness of this photoreactor was demonstrated by measuring the real-time degradation of two model compounds, salicylic acid and methylene blue, in homogeneous and heterogenous systems. Photolysis of MB with H2O2 results in increasing of rate constants as [H2O2] increased. Heterogeneous photocatalysis of MB and SA was fastest achieved in ZnO dosage of 0,20 g.L-1. This mini-photoreactor allows monitoring the real-time kinetic performance collecting almost a thousand points in each experiment, leading to accurate rate constants. Moreover, this system presented positive environmental aspects such as: lower reactants and catalyst amounts, lower cost and waste amounts, use of the UV-LED radiation and labor time saving. This is a novel approach to determine the photoreaction effectiveness and it can be applied to systematic studies especially for the kinetic parameter determinations." @default.
• W2905027424 created "2018-12-22" @default.
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• W2905027424 date "2019-03-01" @default.
• W2905027424 modified "2023-10-16" @default.
• W2905027424 title "Kinetic spectrophotometric method for real-time monitoring of ultraviolet photoreactions: A mini-photoreactor" @default.
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• W2905027424 doi "https://doi.org/10.1016/j.saa.2018.12.033" @default.
• W2905027424 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/30583163" @default.
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