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- W2907337003 abstract "Seven novel aluminium complexes supported by Schiff base ligands derived from o ‐diaminobenzene or o ‐aminothiophenol were synthesized and characterized. The reactions of AlMe 3 with L 1 ( N , N′ ‐bis(benzylidine)‐ o ‐phenylenediamine) and L 2 ( N , N′ ‐bis(2‐thienylmethylene)‐ o ‐phenylenediamine) gave the complexes L 1 AlMe 3 ( 1 ) and L 2 AlMe 2 ( 2 ), respectively, which involved two types of reaction mechanisms: one was proton transfer and ring closure, and the other was alkyl transfer. Complexes L 3 AlMe 2 (HL 3 = 4‐chlorobenzylidene‐ o ‐aminothiophenol) ( 3 ), L 4 AlMe 2 (HL 4 = 2‐thiophenecarboxaldehyde‐ o ‐aminothiophenol) ( 4 ), L 3 AlH(NMe 3 ) ( 5 ), L 4 AlH(NMe 3 ) ( 6 ) and L 5 AlH(NMe 3 ) (HL 5 = 4‐methylbenzylidene‐ o ‐aminothiophenol) ( 7 ) were prepared by reacting HL 3–5 with equimolar AlMe 3 or H 3 Al⋅NMe 3 , respectively. Compounds 3 – 7 feature an organic–inorganic hybrid containing CNAlSC five‐membered ring. All complexes were characterized using 1 H NMR and 13 C NMR spectroscopy, X‐ray crystal structure analysis and elemental analysis. The efficient catalytic performances of 1 – 7 for the hydroboration of carbonyl groups were investigated, with compound 4 exhibiting the highest catalytic activity among all the complexes." @default.
- W2907337003 created "2019-01-11" @default.
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- W2907337003 date "2019-01-02" @default.
- W2907337003 modified "2023-10-15" @default.
- W2907337003 title "Novel aluminium compounds derived from Schiff bases: Synthesis, characterization and catalytic performance in hydroboration" @default.
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- W2907337003 doi "https://doi.org/10.1002/aoc.4637" @default.
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