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- W2907842010 abstract "Triazoles are an important class of N-heterocycles that are well known for their broad biological activities. In this work, we would like to demonstrate a direct synthesis of the rare fused bicyclic [1,2,3]-triazoles, employing γ-N-protected amino diazoketones as useful synthetic platforms. The strategy was based on the deprotection of a trifluoroacetamide group for the intramolecular and in situ generation of an α-diazo imine intermediate, followed by a 5-endo-dig cyclization to construct the bicyclic unit. In this fashion, the synthesis of a series of fused bicyclic [1,2,3]-triazoles could be carried out in good to excellent yields (63–95%)." @default.
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- W2907842010 date "2019-01-03" @default.
- W2907842010 modified "2023-10-18" @default.
- W2907842010 title "Synthesis of Fused Bicyclic [1,2,3]-Triazoles from γ-Amino Diazoketones" @default.
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- W2907842010 doi "https://doi.org/10.1021/acsomega.8b02764" @default.
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