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- W2908413369 abstract "A conceptually novel sulfoxonium metathesis reaction between TMSOI and cost-effective DMSO-d6 is developed for the efficient generation of a new trideuteromethylation reagent TDMSOI. The new reagent TDMSOI is produced highly efficiently by simply heating a mixture of TMSOI and DMSO-d6 and directly used for subsequent trideuteromethylation in a “one-pot” operation. The preparative power of the new versatile reagent and the “one-pot” protocol is demonstrated by its use to install the −CD3 moiety into broad functionalities including phenols, thiophenols, acidic amines, and enolizable methylene units in high yield and at a useful level of deuteration (>87% D)." @default.
- W2908413369 created "2019-01-11" @default.
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- W2908413369 date "2019-01-07" @default.
- W2908413369 modified "2023-10-15" @default.
- W2908413369 title "Trideuteromethylation Enabled by a Sulfoxonium Metathesis Reaction" @default.
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- W2908413369 doi "https://doi.org/10.1021/acs.orglett.8b03641" @default.
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