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• W2908602609 abstract "An efficient analytical method was developed and validated using a modified QuEChERS method and LC-MS/MS for the detection and quantification of neonicotinoid insecticide residues in rice whole grain and rice straw. The samples were extracted using acetonitrile and cleaned up by dispersive solid-phase extraction. Validation based on five fortification levels showed good recoveries of neonicotinoids ranging from 75% to 116 % and 60% to 105 % for rice whole grain and straw, respectively. The precision ranged between 3% and 17 %, and 2% and 10 % for grain and straw, respectively. The limit of detection was from 0.007 to 0.0084 mg kg-1 and 0.005 to 0.15 mg kg-1 and the limit of quantification was in the range of 0.024-0.028 mg kg-1 and 0.016-0.051 mg kg-1 for rice whole grain and rice straw, respectively. Monitoring of farm gate samples indicated that, out of 24 samples, 1 rice whole grain sample was contaminated with thiamethoxam residues (0.07 mg kg-1)." @default.
• W2908602609 created "2019-01-25" @default.
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• W2908602609 date "2019-01-16" @default.
• W2908602609 modified "2023-10-05" @default.
• W2908602609 title "Validation and quantification of neonicotinoid insecticide residues in rice whole grain and rice straw using LC-MS/MS" @default.
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• W2908602609 doi "https://doi.org/10.1080/19440049.2018.1562229" @default.
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