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- W2910019075 abstract "A one-pot synthesis of various 5,10-diaryl-5,10-dihydrophenazines (DADHPs) from diarylamines has been achieved by using an iron-catalyzed C-F amination. Homodimerization of magnesium diarylamides, followed by defluorinative intramolecular cyclization (double ortho C-F amination) in the presence of catalytic FeCl2 and stoichiometric 1,2-dibromoethane, affords the corresponding DADHPs with complete regiocontrol. The unique high reactivity of fluorine over other halogens indicates that amination proceeds via an SNAr mechanism facilitated by iron." @default.
- W2910019075 created "2019-01-25" @default.
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- W2910019075 date "2019-01-10" @default.
- W2910019075 modified "2023-09-29" @default.
- W2910019075 title "Ligand-Free Iron-Catalyzed C–F Amination of Diarylamines: A One-Pot Regioselective Synthesis of Diaryl Dihydrophenazines" @default.
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- W2910019075 doi "https://doi.org/10.1021/acs.orglett.8b03702" @default.
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