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- W2911970515 abstract "A metal–organic perovskite which consists of four-membered-ring ammonium (azetidinium), magnesium, and formate ions [(CH2)3NH2][Mg(HCOO)3] was synthesized. Differential scanning calorimetry revealed a first-order phase transition at Tc = 288 K. Besides a sharp anomaly at Tc, a broad Schottky-type anomaly was observed at 273 K. Temperature dependences of spin–lattice and dipolar spin–lattice relaxation times T1 and T1D were determined. In the low-temperature phase, short and long T1-values were observed. T1D showed a minimum of 0.15 ms at around 220 K, which can be assigned to the ring-puckering motion of the azetidinium cation. Compared with the previously reported zinc analogue [(CH2)3NH2][Zn(HCOO)3], energy separation between the two molecular conformations associated with the ring-puckering motion and inhomogeneity that occurred in the crystals at low temperatures are discussed." @default.
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- W2911970515 date "2019-01-25" @default.
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- W2911970515 title "Ring-Puckering Motion of Azetidinium Cations in a Metal–Organic Perovskite [(CH<sub>2</sub>)<sub>3</sub>NH<sub>2</sub>][M(HCOO)<sub>3</sub>] (M = Zn, Mg)—A Thermal and <sup>1</sup>H NMR Relaxation Study" @default.
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- W2911970515 doi "https://doi.org/10.1021/acs.jpcc.8b11789" @default.
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