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- W291207889 abstract "The title compound was prepared in modest yield by treatment of perfluoroisobutylene (PFIB) in acetonitrile solvent with potassium cyanide in the presence of 18-crown-6 ether catalyst. Product formation in the time course of the reaction was observed to follow a Gaussian rather than a plateau profile; maximum concentration occurred between 60 and 70 min with incomplete conversion of the PFIB. A major by-product of the reaction was tentatively identified as a condensation product of the PFIB and title compound. Reaction mechanisms consistent with experimental results are proposed to explain product and by-product formation. Suggestions for further work are proposed." @default.
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- W291207889 date "1988-05-01" @default.
- W291207889 modified "2023-09-23" @default.
- W291207889 title "New method for the synthesis of perfluoro-beta, beta-dimethylacrylonitrile. Technical report, August-December 1985" @default.
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