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- W2912151819 abstract "Abstract While typical organic azides have long been known to undergo 1–3 dipolar cycloadditions with strained C C multiple bonds, such chemistry has never been reported between organomimetic carboranyl azides and alkenes. Here we show that the carborane o-PhCN3CB10H10 readily undergoes cycloaddition with norbornene at ambient temperature to afford the corresponding triazole adduct with perfect exo-selectivity. The structure of the ensuing heterocycle was unambiguously determined by multinuclear NMR, correlation NMR, and single crystal X-ray diffraction experiments. This first example of such reactivity demonstrates a method to easily introduce carborane clusters directly to scaffolds of interest, without having an organic spacer between the azide functionality and cluster." @default.
- W2912151819 created "2019-02-21" @default.
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- W2912151819 date "2019-03-01" @default.
- W2912151819 modified "2023-10-12" @default.
- W2912151819 title "The first example of a “click” reaction with a carboranyl azide and an olefin" @default.
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- W2912151819 doi "https://doi.org/10.1016/j.tet.2019.01.049" @default.
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