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• W2912159368 startingPage "6385" @default.
• W2912159368 abstract "Abstract Direct amination of C(sp 3 )−H bonds is of broad interest in the realm of C−H functionalization because of the prevalence of nitrogen heterocycles and amines in pharmaceuticals and natural products. Reported here is a combined electrochemical/photochemical method for dehydrogenative C(sp 3 )−H/N−H coupling that exhibits good reactivity with both sp 2 and sp 3 N−H bonds. The results show how use of iodide as an electrochemical mediator, in combination with light‐induced cleavage of intermediate N−I bonds, enables the electrochemical process to proceed at low electrode potentials. This approach significantly improves the functional‐group compatibility of electrochemical C−H amination, for example, tolerating electron‐rich aromatic groups that undergo deleterious side reactions in the presence of high electrode potentials." @default.
• W2912159368 created "2019-02-21" @default.
• W2912159368 creator A5074617275 @default.
• W2912159368 creator A5077272675 @default.
• W2912159368 date "2019-03-14" @default.
• W2912159368 modified "2023-10-16" @default.
• W2912159368 title "Merging Photochemistry with Electrochemistry: Functional‐Group Tolerant Electrochemical Amination of C(sp³)−H Bonds" @default.
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• W2912159368 doi "https://doi.org/10.1002/anie.201813960" @default.
• W2912159368 hasPubMedCentralId "https://www.ncbi.nlm.nih.gov/pmc/articles/6482061" @default.
• W2912159368 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/30763466" @default.
• W2912159368 hasPublicationYear "2019" @default.
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