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- W2912222711 abstract "Although helium pycnometry is generally the method of choice for skeletal density measurements of porous materials, few studies have provided a wide range of case studies that demonstrate how to best interpret raw data and perform measurements using it. The examination of several different classes of materials yielded signature traits from helium pycnometry data that are highlighted. Experimental parameters important in obtaining the most precise and accurate value of skeletal density from the helium pycnometer are as high as possible percent fill volume and good thermostability. The degree of sample activation is demonstrated to affect the measured skeletal density of porous zeolitic, carbon, and hybrid inorganic–organic materials. In the presence of a significant amount of physisorbed contaminants (water vapor, atmospheric gases, residual solvents, etc.), which was the case for ZSM-5, MIL-53, and F400, but not ZIF-8, the skeletal density tended to be overestimated in the low percent volume region. In ad..." @default.
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- W2912222711 date "2019-01-30" @default.
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- W2912222711 title "Understanding Material Characteristics through Signature Traits from Helium Pycnometry" @default.
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- W2912222711 doi "https://doi.org/10.1021/acs.langmuir.8b03731" @default.
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