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- W2912262355 abstract "In this research, 5‐benzoyl‐6‐phenyl‐4‐(4‐trifluoromethylphenyl)‐2‐{oxo and thioxo}‐3,4‐dihydro‐1 H ‐pyrimidines ( 1 , 2 ) were synthesized by using multicomponent cyclocondensation reaction under microwave irradiation and classical heating. Compounds 3 , 4 , 6 , 7 , and 8 obtained reactions of 5‐benzoyl‐6‐phenyl‐4‐(4‐trifluoromethylphenyl)‐2‐thioxo‐3,4‐dihydro‐1 H ‐pyrimidine ( 1 ) and acetic anhydride, diethyl 2‐bromomalonate, bromoacetic acid, 3‐bromopropionic acid, methyl iodide, respectively. Compound 4 was both acetylated and hydrolyzed in acetic acid to give compound 5 . The structures of all compounds were determined by using spectroscopic techniques like FT‐IR, 1 H/ 13 C NMR, and elemental analyses, and the structures of compounds 1 and 3 were analyzed by X‐ray crystal analysis. In addition, the quantum chemical parameters and full geometry optimizations for all compounds were computed using density functional theory based on B3LYP and the 6‐31G (d, p) basis set." @default.
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- W2912262355 date "2019-01-29" @default.
- W2912262355 modified "2023-10-16" @default.
- W2912262355 title "A Green Protocol for Simple One‐pot Synthesis of New Pyrimidine Derivatives Both Microwave Irradiation and Conventional Heating: Reactions, Characterization, and Theoretical Calculations" @default.
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- W2912262355 doi "https://doi.org/10.1002/jhet.3483" @default.
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