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- W2912268335 abstract "We investigated and developed a practical and continuous production of monosilane via parallel reactions in a single molten salt bath consisting of electrolysis of LiCl, hydrogenation of Li and a chemical reaction of LiH and SiCl4. In the normal electrolysis, a bypass current is generated due to Li attached at the anode chamber and at the diaphragm. This bypass current caused production problems and efficiency degradation. We were able to substantially minimize this current by moving the attached Li away from these surfaces electrolytically and by blowing chlorine aimed at the displaced Li during electrolysis. When the electrolysis was performed at 1000 A, this method yielded current efficiencies of electrolysis and eventual monosilane generation of 97.5% and 92%, respectively." @default.
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- W2912268335 date "1987-01-01" @default.
- W2912268335 modified "2023-10-18" @default.
- W2912268335 title "A Method for Continuous Monosilane Generation Utilizing Molten Salt Electrolysis" @default.
- W2912268335 doi "https://doi.org/10.1149/198707.0939pv" @default.
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