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- W2912382073 abstract "Abstract Wir berichten über die Festkörperstrukturen von Bis(nonafluor‐tert‐butyl)peroxid [(F 3 C) 3 CO] 2 und Bis(undecafluor‐2‐methyl‐2‐butyl)peroxid [(C 2 F 5 )(F 3 C) 2 CO] 2 . Diese Peroxide wurden über die Reaktion des jeweiligen Hypofluorits mit fluorierter Silberwolle dargestellt. Ihre nach In‐situ‐Kristallisation erhaltenen Strukturen weisen aufgrund der sterisch anspruchsvollen Perfluoralkylgruppen ungewöhnliche COOC‐Diederwinkel von 180°, sowie verlängerte O‐O‐Abstände auf. Die perfluorierten Alkylperoxide sind weder schock‐ (>40 J) noch reibungsempfindlich (>360 N). Darüber hinaus reagieren sie nicht mit Halogensäuren (HX, X=F, Cl, Br, I) oder elementaren Halogenen (X 2 ). Ferrocen wird von [(F 3 C) 3 CO] 2 zu [Fe III Cp 2 ] [OC(CF 3 ) 3 ] oxidiert." @default.
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- W2912382073 date "2019-02-18" @default.
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- W2912382073 title "Keine Scheu vor perfluorierten Peroxiden: Synthese und Strukturen von überraschend inerten Perfluoralkylperoxiden" @default.
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- W2912382073 doi "https://doi.org/10.1002/ange.201814417" @default.
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