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• W2912383852 abstract "Abstract A simple, efficient and eco‐friendly method has been developed for the synthesis of biologically active alkyl derivatives of 6‐acetyl‐2 H ‐benzo[ e ][1,3]oxazine‐2,4(3 H )‐dione by using microwave irradiations. The N‐alkylation of 6‐acetyl‐2 H ‐benzo[ e ][1,3]oxazine‐2,4(3 H )‐dione with substituted alkyl derivatives under microwave radiations in presence of Tetra‐n‐butyl ammonium bromide as a phase transfer catalyst to give the desired products. Comparison between conventional and microwave‐assisted synthesis revealed that it reduced the reaction time, improve the yield and purity of 6‐acetyl‐3‐(substituted alkyl)‐2 H ‐benzo[ e ][1,3]oxazine‐2,4(3 H )‐diones analog molecules. All the final compounds were characterized by FT‐IR, 1 HNMR, 13 CNMR, HRMS and Mass spectroscopic analysis, also succeeded to develop and analyze the single crystal XRD of compound 4 f. The antimicrobial evaluation studies show moderate activities against used microbes." @default.
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• W2912383852 date "2019-02-05" @default.
• W2912383852 modified "2023-09-26" @default.
• W2912383852 title "Rapid, Simple and Efficient Microwave‐Assisted Alkylation of 6‐Acetyl‐2<i>H</i>‐Benzo[e][1, 3] Oxazine‐2, 4(3<i>H</i>)‐Dione" @default.
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• W2912383852 doi "https://doi.org/10.1002/slct.201803607" @default.
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