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- W2912448255 abstract "ABSTRACT This study describes a novel and facile synthesis strategy for a styrene‐butadiene rubber (SBR)‐like polymer via Friedel–Crafts‐type reaction between aromatic compounds and polybutadiene using an aluminum chloride as a catalyst. Although gelation was induced by a reaction of a generated carbocation with olefins in other polybutadiene chains in benzene and toluene because of their low electron densities on their rings, anisole with a higher electron density reacted with the polybutadiene carbocation efficiently. The introduction ratio of anisole increased as the reaction proceeded, and the obtained polymer, BRAN polymer, contained 15% anisoles for olefins in the polybutadiene in 4 h at 80 °C as estimated by 1 H NMR analysis. The glass‐transition temperature ( T g ) of the BRAN polymer also increased with anisole content ( T g ~−50 °C when anisole contents 20%). The vulcanizate containing the BRAN polymer showed higher mechanical properties compared to samples using other matrix polymers. © 2019 Wiley Periodicals, Inc. J. Polym. Sci., Part A: Polym. Chem. 2019 , 57 , 841–847" @default.
- W2912448255 created "2019-02-21" @default.
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- W2912448255 date "2019-02-14" @default.
- W2912448255 modified "2023-09-30" @default.
- W2912448255 title "Synthesis of novel diene polymer via friedel-crafts-type reaction of polybutadiene with aromatic compounds" @default.
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- W2912448255 doi "https://doi.org/10.1002/pola.29335" @default.
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