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• W2912454675 abstract "Abstract A zirconium/nickel‐mediated one‐pot synthesis of ketones is reported. In the presence of Zn or Mn, Cp 2 ZrCl 2 was found to dramatically accelerate the coupling and suppress side product formation via an I→SPy displacement at the same time. Unlike Zn/Pd‐ and Fe/Cu‐mediated one‐pot ketone syntheses, the new method is effective for nucleophiles bearing OR or equivalent functional groups at the α‐position. A mechanism comprising a nickel catalytic cycle, a zirconium catalytic cycle, and Zr→Ni transmetalation is proposed, and Cp 2 ZrCl 2 and/or low‐valent Zr species are suggested to play crucial dual roles." @default.
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• W2912454675 date "2017-07-28" @default.
• W2912454675 modified "2023-09-30" @default.
• W2912454675 title "Zirconium/Nickel-Mediated One-Pot Ketone Synthesis" @default.
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• W2912454675 doi "https://doi.org/10.1002/ange.201705520" @default.
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