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- W2912759711 abstract "Der Flash-Kristallisationsprozess ist ein neuartiges Verfahren mit dem gezielt feine Kristalle von gut loslichen Stoffsystemen hergestellt werden konnen. Die Eignung eines Stoffsystems fur diesen Prozess hangt stark von der Keimbildung und der Wachstumgskinetik ab. Es wird eine einfache und schnelle Methode zur Charakterisierung von Stoffsystemen hinsichtlich deren Eignung fur die Flash-Kristallisation vorgestellt. Durch die Bestimmung von Induktionszeiten wird zunachst ein Uberblick uber das Kristallisationsverhalten der Stoffsysteme gewonnen. Weiterhin wird ein Modell zur gezielten Auslegung von Flash-Versuchen bei unterschiedlichen Bedingungen prasentiert. Die Analyse der Produktsuspension erlaubt schlieslich eine Beurteilung, ob eine Flash-Kristallisation durchgefuhrt werden kann.Flash crystallization is a newly developed process to produce small, fine crystals from solutions of rather well soluble substances. Since the suitability of a substance depends largely on nucleation and growth kinetics, not all combinations of solute and solvent are applicable to this process. Therefore, a simple and fast method to check the suitability of a system is presented. As a first step, an overview about the crystallization behavior of the solute-solvent systems is gained by measuring induction times. Furthermore, a model is presented that enables the design of flash experiments for different process parameters. Finally, an analysis of the product suspension allows for the evaluation of a solute-solvent system with regard to the feasibility of the flash crystallization process." @default.
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- W2912759711 date "2016-04-07" @default.
- W2912759711 modified "2023-09-24" @default.
- W2912759711 title "Flash-Kristallisation" @default.
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- W2912759711 doi "https://doi.org/10.1002/cite.201500148" @default.
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