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- W2912797739 abstract "Significance We present a comprehensive quantitative study of the dynamic order–disorder phase transition of Pt 3 Co nanoparticles, binary intermetallic oxygen-reduction reaction fuel cell electrocatalysts, during postsynthesis annealing. We employed in situ synchrotron-based X-ray diffraction (XRD) and in situ scanning transmission EM (STEM) to study the phase transition and morphological and structural changes during real-time annealing. In situ XRD revealed the impact of annealing/cooling conditions on the degree of ordering, particle size and lattice strain. In situ heating STEM enabled visualization of nanoparticle migration and growth. We find that a higher degree of ordering leads to more active and durable electrocatalysts. Our findings represent a groundbreaking advance in electrocatalyst development/design with a broad impact on energy materials, in general, and fuel cells, in particular." @default.
- W2912797739 created "2019-02-21" @default.
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- W2912797739 date "2019-01-22" @default.
- W2912797739 modified "2023-10-14" @default.
- W2912797739 title "Revealing the atomic ordering of binary intermetallics using in situ heating techniques at multilength scales" @default.
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- W2912797739 doi "https://doi.org/10.1073/pnas.1815643116" @default.
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