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- W2913176772 endingPage "100221" @default.
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- W2913176772 abstract "Grain boundary engineering (GBE) in FCC alloys relies on the presence of low-energy, coherent Σ3 boundaries to improve material performance. To make microstructures with a profuse network of Σ3 boundaries, a repetitive cycle of low-level deformation and followed by annealing is commonly employed. In this work, we use a combination of in situ SEM, in situ TEM, and a relaxation theory for grain boundaries to investigate the structural states of grain boundaries in Cu after a cycle or many cycles of deformation and annealing steps. It is revealed that during annealing the orientation relationships and boundary morphology of deformed Σ3 and higher order variants, Σ9 boundaries, change appreciably, from being curved to distinctly, crystallographically faceted. The theoretical analysis identifies the faceting process and the crystallography of the facets as corresponding to the optimal, low-energy structures for the observed orientation relationships. It is, therefore, shown that post-deformation heat treatments used in GBE are recovering the highly deviated and deformed Σ3s boundaries to a low-energy state." @default.
- W2913176772 created "2019-02-21" @default.
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- W2913176772 date "2019-03-01" @default.
- W2913176772 modified "2023-10-01" @default.
- W2913176772 title "Determination of minimal energy facet structures in Σ3 and Σ9 grain boundaries: Experiment and simulation" @default.
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- W2913176772 doi "https://doi.org/10.1016/j.mtla.2019.100221" @default.
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