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- W2917133912 abstract "Solvent extraction methods were investigated as an analytical technique for Ce- Cu- Pu alloys. Analysis of Fe-- Pu alloys proved that Pu III-o- phenanthroline complexes (if formed at all) do not interfere with spectrophotometric Fe determination at 515 millimicrons. A controlled potential coulometric method in which Fe is analyzed in the presence of Pu because of a suitable separation in the oxidationreduction potentials was developed and tested with encouraging results. A high temperature calorimeter for measuring specific and latent heats in phase transformations of potential Pu fuel systems and for determining thermal conductivities was aiso developed. The thermal conductivity of Ni was measured in agreement with other determinations. An induction-coupled plasma torch producing temperatures up to 20,000 deg K and permitting melting of ceramics in inert, oxidizing, or reducing atmospheres was used to produce contamination-free microspheres of PuO/sub 2/ and Pu-bearing oxidation were also produced. Phase equilibria, solidus temperatures, boundary intersections, ternary phase diagrams, and liquidus temperatures were among the aspects studied in analyses of Ce-- Co-- Pu, CeCu/sub 6/-- Pu/sub 4/Cu/sub 17/, and Ce- Ni-- Pu systems. Pu/U homogeneity was investigated for UC-- PuC systems; the concentration of Ni added to this system as a sintering aid was alsomore » examined. The viscosities of some Ce-- Co- Pu alloys were measured by an absolute method from their melting points to 1000 deg C in an oscillating-cup viscosimeter. Zirconium oxide viscosity capsule liners were evaluated for measuring the viscosity of Bi and were found acceptable. Zirconia liners can also be used for liquid Pu alloy measurements up to 1300 deg C. (D.C.W.)« less" @default.
- W2917133912 created "2019-03-02" @default.
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- W2917133912 date "1963-05-29" @default.
- W2917133912 modified "2023-09-24" @default.
- W2917133912 title "REACTOR FUELS AND MATERIALS DEVELOPMENT. PLUTONIUM RESEARCH, JANUARY- MARCH 1963" @default.
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