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• W2917925046 abstract "Palladium doped anatase TiO2 nanoparticles were synthesised by a rapid (3 min) one-pot microwave synthesis technique at low temperature and pressure. After being fully characterised by SEM, XRD, Raman, XPS and EDX, photocatalytic nitrate reduction and ammonia production were studied over various dopant levels between 0-3.97 wt% Pd and compared to similar previous literature. Improved yields of ammonia were observed with most dopant levels when compared to non-doped microwave synthesised TiO2 with 2.65 wt% found to be the optimum dopant level producing 21.2 μmol NH3. Electrochemical impedance spectroscopy of TiO2 and Pd-TiO2 photoelectrodes revealed improvements in charge transfer characteristics at high Pd dopant levels." @default.
• W2917925046 created "2019-03-02" @default.
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• W2917925046 date "2019-01-01" @default.
• W2917925046 modified "2023-10-01" @default.
• W2917925046 title "Microwave synthesised Pd–TiO₂ for photocatalytic ammonia production" @default.
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• W2917925046 doi "https://doi.org/10.1039/c8ra09762c" @default.
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