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- W2919588196 abstract "2-Methylbenzothiazole is widely used as the half-product for the thiocyanine dyes photosensitisers synthesis. It usually is synthesized by action of an acetic anhydride in excess on 2-mercaptoaniline. High-temperature reaction of 2-mercaptoaniline derivatives with the organic acids at temperatures above 200oC was extensively studied, but the reaction with acetic acid was not described [1-5]. The method of benzothiazole and its lower 2-alkylsubstituted derivatives synthesis from zinc 2-aminomercaptide and lower aliphatic acids was earlier described, but even in this paper in the examples of 2-methylbenzothiazole synthesis acetic anhydride alone or its mixture with benzene was used [6]. We have elaborated a new efficient method of 2-methylbenzothiazole synthesis from 2-mercaptoaniline and acetic acid shown at the scheme 1" @default.
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- W2919588196 date "1999-11-01" @default.
- W2919588196 modified "2023-09-27" @default.
- W2919588196 title "2-Methylbenzothiazole synthesis from 2-Mercaptoaniline and Acetic Acid" @default.
- W2919588196 doi "https://doi.org/10.3390/ecsoc-3-01732" @default.
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