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- W2920241542 abstract "The synthesis of P-stereogenic aminophosphine-boranes has been developed on the basis of umpolung reactivity of in situ generated alkylarylphosphido-boranes, which are normally configurationally unstable intermediates. In our case, their high configurational stability was due to the slow release of the hydroxyalkyl protecting group, together with the fast formation of the iodophosphanylborane in the presence of N-iodosuccinimide. The subsequent substitution reaction was found to proceed in moderate to good yields and in a very high stereospecifity (es) using a variety of amines as nucleophiles." @default.
- W2920241542 created "2019-03-11" @default.
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- W2920241542 date "2019-02-28" @default.
- W2920241542 modified "2023-10-14" @default.
- W2920241542 title "Umpolung Reactivity of in Situ Generated Phosphido-Boranes: An Entry to P-Stereogenic Aminophosphine-Boranes" @default.
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- W2920241542 doi "https://doi.org/10.1021/acs.joc.9b00333" @default.
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