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- W2920804959 abstract "We describe the evolution of a synthetic strategy for the construction of the marine polyketide salimabromide. Combining a bicyclo[3.1.0]hexan-2-one ring-expansion to build up a functionalized naphthalene and an unprecedented rearrangement/cyclization cascade, enabled synthesis of a dearomatized tricyclic subunit of the target compound. Alternatively, an intramolecular ketiminium [2+2]-cycloaddition and subsequent Baeyer-Villiger ring-expansion gave access to the sterically encumbered architecture of salimabromide. Sequential oxidation of the carbon framework finally enabled the total synthesis of this unusual natural product." @default.
- W2920804959 created "2019-03-22" @default.
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- W2920804959 date "2019-06-01" @default.
- W2920804959 modified "2023-10-10" @default.
- W2920804959 title "Ring-expansion approaches for the total synthesis of salimabromide" @default.
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- W2920804959 doi "https://doi.org/10.1016/j.tet.2019.03.010" @default.
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