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• W2921812662 abstract "A novel Mo-Ag-S cubane-like complex, {MoAg3S3Cl}(PPh3)3S, has been synthesized from AgCl, PPh3 and MoS42− in appropriate conditions. Crystallographic data for C54H45ClP3Ag3S4Mo: Mr = 1370.1, monoclinic, space group P21/c, a = 15.78(2), b = 11.239(6), c = 30.38(2) Å, β = 93.16(6)°, U = 5380(7) Å3; Z = 4; Dcalc = 1.69 g cm−3 μ = 16.11 cm−1; T = 296 K; λ (Mo Kα) = 0.71069 Å, 2θmax = 50.1°. Final R = 0.050 for 5698 observed reflections with I>3σ(I) and 595 variables. The unit cell contains four discrete neutral molecules. The molecular comprises one cubane-like cluster core {MoAg3S3Cl}2+, three PPh3 ligands attached to each Ag atoms and one terminal sulfido ligand attached to the Mo atom at 2.103(3) Å. The mean distance between the Mo and Ag atoms is 2.944(2) Å which is too long to effectively bond. The bond lengths of the three Ag-Cl bonds are in the same range and average 2.815(3) Å." @default.
• W2921812662 created "2019-03-22" @default.
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• W2921812662 date "1992-01-01" @default.
• W2921812662 modified "2023-09-23" @default.
• W2921812662 title "The synthesis and crystal structure of a first cubane-like complex of the Mo-Ag-S series: {MoAg3S3Cl}(PPh3)3S" @default.
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• W2921812662 doi "https://doi.org/10.1016/s0020-1693(00)80328-x" @default.
• W2921812662 hasPublicationYear "1992" @default.
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