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- W2922411385 abstract "There is an increasing interest in investigating how polyfluorination of carbohydrates modifies their physical and biological properties. An example that has caught much attention is 2,3,4-trideoxy-2,3,4-trifluoroglucose. Four syntheses of this compound have been reported, which are either low yielding or long (13 or more steps). We report a 6-step synthesis of 2,3,4-trideoxy-2,3,4-trifluoroglucose starting from levoglucosan. The solution-phase structure of an intermediate, 1,6-anhydro-2,4-dideoxy-2,4-difluoroallose, features a rare example of a bifurcated F···H(O)···F hydrogen bond and is compared to its crystal structure." @default.
- W2922411385 created "2019-03-22" @default.
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- W2922411385 date "2019-03-14" @default.
- W2922411385 modified "2023-10-12" @default.
- W2922411385 title "Synthesis of 2,3,4-Trideoxy-2,3,4-trifluoroglucose" @default.
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- W2922411385 doi "https://doi.org/10.1021/acs.joc.9b00310" @default.
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