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- W2922786625 abstract "Abstract Novel eight-membered 1,5-dibenzyl-1,2,5,6-tetrahydro-1,5-diazocines (4a-4f) were prepared by a new three-component aza-annulation as one-pot method from paraformaldehyde, ethyl propiolate, and benzylamine. Unique structure of products, an easy experimental workup, the use of simple and available starting materials, and the high atom economy are the main advantages of this method. The target compound was isolated and unambiguously confirmed by NMR spectra (1D-NMR and 2D-NMR), high-resolution mass spectrometry, and single-crystal X-ray diffraction analysis. Furthermore, the products possess N-benzyl-protected secondary amines and β-enamine esters, which can serve in further functionalizations to produce molecular diversity for use in medicinal and synthetic chemistry." @default.
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- W2922786625 date "2019-07-01" @default.
- W2922786625 modified "2023-10-16" @default.
- W2922786625 title "Synthesis, NMR analysis and X-ray crystal structure of novel 1,5-dibenzyl-1,2,5,6-tetrahydro-1,5-diazocines" @default.
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- W2922786625 doi "https://doi.org/10.1016/j.molstruc.2019.03.079" @default.
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