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• W2923996890 abstract "A rapid UPLC-MS/MS method for the determination of tamoxifen (TAM), N-desmethyltamoxifen, 4-hydroxytamoxifen and endoxifen in human plasma was validated, after a simple protein precipitation.The analysis was achieved on a C18 analytical column, using a gradient elution with a mobile phase of water and acetonitrile for 4.5 min.The validated method demonstrated good linearity between 1 and 500 ng/ml for TAM and N-desmethyltamoxifen; between 0.2 and 100 ng/ml for endoxifen and between 0.1 and 50 ng/ml for 4-hydroxytamoxifen. The method also provided satisfactory results in terms of within day and between day imprecisions and accuracy, and also in terms of time stability and specificity.The method is applied routinely for TAM monitoring from patients undergoing therapy." @default.
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• W2923996890 date "2019-06-01" @default.
• W2923996890 modified "2023-10-02" @default.
• W2923996890 title "New UPLC–MS/MS assay for the determination of tamoxifen and its metabolites in human plasma, application to patients" @default.
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• W2923996890 doi "https://doi.org/10.2144/fsoa-2018-0113" @default.
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