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• W2924835712 abstract "Abstract A new glycoluril derivative‐1 H , 4 H , 5 H , 8 H ‐2, 3a, 4a, 6, 7a, 8a‐hexaazacyclopenta[ def ]fluorene‐4, 8‐dione, hexahydro‐2, 6‐bis(phenylmethyl) ( 3 ) is strategically designed and synthesized through the reaction between glycoluril, formaldehyde and benzylamine with the optimized molar ratio of 1:6:2. Compound 3 is fully characterized by 1 H NMR, 13 C NMR, IR, MS and X‐ray single crystal diffraction. Reduction of compound 3 delivers a potential precursor‐imidazo[4, 5‐ d ]imidazole, octahydro‐hexahydro‐2, 6‐bis(phenylmethyl) ( 4 ) for the synthesis of novel nitramine explosives (i.e. bicyclo‐HMX and bi‐RDX). The nitration and hydrolysis of compound 4 are investigated in detail and three ring‐opened molecules N , 2, 4‐trinitro‐benzenemethanamine ( 8a ), N , 2‐dinitro‐benzenemethanamine ( 8b ) and N ‐methylene‐benzenemethanamine ( 9 ) are obtained." @default.
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• W2924835712 date "2019-03-26" @default.
• W2924835712 modified "2023-09-25" @default.
• W2924835712 title "Synthesis, Hydrolysis, Reduction and Nitrolysis of Glycoluril‐Derived Precursors: Another Attempt toward the Synthesis of Nitramine Explosives" @default.
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• W2924835712 doi "https://doi.org/10.1002/slct.201900204" @default.
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