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• W293051377 abstract "The preparations are described of the unstable allyl-, pseudo-allyl- and benzyl- complexes of formula RReO3 (R = C3H5-, CH2CMeCH−, CH2CHCHCHCH2−, C2H5OC(O)CH2−, PhCH2− from Re2O7 and the tin reagents RSn(n-Bu)3. In situ-NMR studies show that the allylic species exhibit η1-coordination. The vinyl analogue (CH2CMe)ReO3 is prepared from Re2O7 and Zn(CMeCH2)2. Quinuclidine adducts of type RReO3 · Quin are also reported. Decomposition studies of the allyl and 1-methallyl derivatives show concentration-dependent radical pathways in anhydrous solution (1,5-hexadiene and propene evolution) and facile hydrolysis (propene evolution) at low temperature. Allyltrioxorhenium(VII) does not react with oxygen, while peroxides predominantly yield 2-propen-1-ol." @default.
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• W293051377 date "1994-11-01" @default.
• W293051377 modified "2023-10-17" @default.
• W293051377 title "Multiple bonds between main-group elements and transition metals" @default.
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• W293051377 doi "https://doi.org/10.1016/0022-328x(94)85030-5" @default.
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